Introduction
45 steel is a medium carbon steel commonly used in engineering components, such as gears, shafts and fasteners. It provides good wear resistance and excellent toughness at elevated temperatures. In this experiment, the grain morphology of 45 steel (900℃ water quenched) will be evaluated by an optical and scanning electron microscopy (SEM).
Experimental Procedures
A sample of 45 steel was cut into a reduced section (3 mm thick x 30 mm wide). The sample was then heated in a furnace up to 900℃, and quenched in water. The sample was either polished and etched with a nital etchant (2%) to reveal grain morphology.
The sample was then observed under an optical microscope (Nikon) with a magnification up to 500x. The sample was then placed in the SEM in order to observe the microstructure of the steel at a high magnification.
Results and Discussion
The optical micrograph of the sample (see fig.1) revealed a ferrite-like structure with a matrix of small grains having a mean size of ~ 2 µm. In addition, there were also some larger grains (about 10-20 µm) dispersed throughout.
Figure 2 is the scanning electron microscopy micrograph of the sample. It can be seen that the grain structure of the steel consisted of a matrix of small grains with an average size of 2µm. The larger grains (10-20µm) appeared to be more rounded, indicating a higher temperature treatment of the steel.
Conclusion
The microstructure of the 45 steel revealed by optical and SEM showed the presence of ferrite-like structure with a matrix of small grains with a mean size of ~ 2 µm, and some larger grains (about 10-20 µm) dispersed throughout. This indicates that the steel was water quenched from 900℃, which caused the larger grains to be more rounded.