Introduction
Metallographic analysis of 45# steel (powder carburizing) are provided in this paper to obtain information on microstructural details. This experiment includes sample preparation, optical metallography, and microstructure analysis.
Materials and Method
For this experiment, 45# steel powder that has been carburized was obtained.
Sample Preparation
The sample was cleaned then polished with an angel grinder to create a mirror finish on the sample.
Polishing with SiC
SiC was then used to polish the sample after the mirror finishing. A diamond paste was then used to promote finer polishing.
Polishing with Alumina
Alumina paste was then used to polishing the sample after the polishing with diamond paste.
Metal Etching
The sample was etched for five minutes with Nital etchant to reveal its microstructure.
Metallographic Analysis
An optical microscope was used in order to observe and take pictures of the etched sample.
Results and Discussion
The microstructure of the sample is shown in the figure 1. The microstructure consists mainly of martensite along with a small amount of ferrite. The martensite is characterized by its needle-like morphology and is formed by quenching and transformation (Q&T) of austenite. The small amount of ferrite observed is a result of the decomposition of martensite during the cooling process.
Figure 1. Microstructure of the 45# steel powder carburized sample.
Conclusion
Metallographic analysis of 45# steel powder carburized sample was carried out in this paper. Sample preparation, optical metallography, and microstructure analysis were performed. The microstructure of the sample was observed and consisted mainly of martensite and a small amount of ferrite. The results showed that the Q&T process during the carburizing process produced the needle-like morphology of martensite and the decomposition of martensite during cooling produced the small amount of ferrite.