The microhardness, composition and fraction and morphology of the as-quenched cobalt-containing iron-chromium-nickel alloys (930°C × 1h oil-quenched) were studied for the study of microstructure of the alloys. The cobalt-containing iron-chromium-nickel alloys were obtained from the vacuum arc melting (VAR) process.
The microhardness of the as-quenched cobalt-containing iron-chromium-nickel alloys was measured at room temperature. The results showed that the microhardness increased with increased time of oil quenching. The maximum microhardness of the as-quenched alloy was obtained after 2.5 h oil quenching. There was no significant difference in microhardness between the 1 h oil quenched and the 2.5 h oil quenched alloys.
The composition and fraction of the as-quenched cobalt-containing iron-chromium-nickel alloys were also studied. The results showed that the cobalt content decreased with increased time of oil quenching. The highest cobalt content was observed at 1 h oil quenching and then decreased progressively with increasing the oil quenching time beyond 1 h. The fraction of the alloy elements (iron, chromium, nickel, and cobalt) also decreased with increased oil quenching time, except for iron and cobalt.
The morphology of the as-quenched cobalt-containing iron-chromium-nickel alloys was also studied. The alloys were observed under an optical microscope, scanning electron microscope (SEM) and transmission electron microscope (TEM). The optical microscopy revealed that the as-quenched alloys had a granular microstructure. The SEM micrograph showed that the alloys had a dendritic microstructure. The TEM micrographs showed that the alloys had a very fine microstructure and small particles were also present in the microstructure.
The microstructure of the as-quenched cobalt-containing iron-chromium-nickel alloys was affected by the oil quenching temperature and treatment time. It was found that the microhardness of the as-quenched alloys was affected by the cobalt content, which decreased with increasing the oil quenching time beyond 1 h. The composition and fraction of the alloy elements also decreased with increasing the quenching time beyond 1 h. The optical, SEM and TEM micrographs showed that the alloys had a granular and dendritic microstructure. The alloys also had a very fine microstructure and small particles were present in the microstructure.