18Cr2Ni4WA is a cast austenitic heat-resistant steel with good metallurgical properties and reasonable mechanical properties. This steel is commonly used for components operating at temperatures up to 950°C in the aerospace, power generation and nuclear industries.
The microstructure of this steel can be analysed using a quantitative analysis of grains and possible growth structures. Qualitatively, the analysis consists primarily of determining the composition, abundance, size and shape of individual grains and their components.
Grain size of 18Cr2Ni4WA can be determined by taking a standard metallographic sample and etching it in a suitable etchant. The etched sample is then observed under a microscope and image analysis is performed to determine grain size, shape, orientation and boundary distributions.
The amount of impurities present in the steel can be quantified by preparing a polished sample and viewing it under a scanning electron microscope. This analysis can reveal the type and concentration of inclusions present.
To determine the grain boundaries and the amount of segregation present in the sample, an optical microscope can be used. This microscope is capable of magnifying the sample up to 500X, allowing for a more detailed view of grain boundaries and other structural defects.
A closer look at the microstructure can be obtained using X-ray diffraction (XRD) techniques. XRD techniques detect light reflected from crystal planes, allowing for the determination of crystal plane orientation and the presence of any impurities or segregations.
Similarly, transmission electron microscopy (TEM) can be used to analyse the microstructure of 18Cr2Ni4WA. TEM is capable of providing detailed information on the existence of defects, impurities, segregation and grain boundaries.
In summary, analysis of the metal structure of 18Cr2Ni4WA can be completed using a variety of techniques. These techniques allow for a more detailed understanding of the metal’s properties and its suitability for different applications.