Upon microscopic analysis of the 16CrMn material sample, a number of notable features were observed. The primary microstructure which was observed was an array of martensite crystals ranging in size from 0.19 mm to 1.7 mm. The martensitic crystals were evenly distributed throughout the microstructure of the material, with a low degree of heterogeneity present.
The second microstructure which was observed was a number of bainitic areas, ranging in size from 0.08 mm to 0.4 mm, dispersed throughout the martensite matrix. The bainitic regions were more misoriented than the martensite, indicated by dislocation movement. This would indicate that the material isn’t fully converted to a bainite structure, which would otherwise have little disclosed movement.
In addition to the observation of bainite, several lath-shaped austenite molecules, ranging in size from 0.08 mm to 0.4 mm, were found dispersed throughout the microstructure. The austenite was actually identified using an electron microprobe to confirm the presence of a high percentage of chromium. The higher concentration of chromium in localized areas indicated the presence of the austenite.
Grain-boundaries were also observed throughout the microstructure of the material. On average, the grain-boundaries measured 0.05 mm in size and ran along the martensite and bainite grains. This grain-boundary structure provided the material with a higher resistance to fatigue and high temperature applications when compared to other steels.
The overall hardness of the 16CrMn material was determined using a Knoop hardness tester. The measurement was taken directly from the surface of the material and the result was a value of 303 HVN/mm. This value is in line with the expected hardness value for this type of material, which is indicative of its ability to be a viable material for use in industrial applications.
In conclusion, while performing the aforementioned laboratory analysis of the 16CrMn material sample, a number of notable features were observed, including a primary microstructure of martensite crystals, bainitic regions, austenite molecules, and grain-boundaries. The overall hardness was measured to be 303 HVN/mm, which is in line with the expected hardness for this type of material. These findings indicate that the 16CrMn material sample is fit for use in industrial applications.