Sintering Neck
Sintering neck is a phenomenon that is usually the result of incorrect temperatures, timeframes, and / or powder properties when powder metallurgy is used. It typically has two sources associated with it: (1) high green compacted compact hardness or high shear strength of a given material; and (2) unbalanced or improperly sized particles within a given particle population. Sintering neck can appear as misaligned holes, burrs, or other types of defects at the base of the part or at the location of the sintering furnace.
High Green Compacted Compact Hardness or High Shear Strength
High green compacted compact hardness or high shear strength occurs when the intense pressure of vibration that is imparted during a compaction cycle is greater than the compressibility of the material. This results in a blunting of the real corners, resulting in a higher than normal green hardness in the compacts. As a result, in the subsequent sintering and debinding cycle, the high green hardness may cause non-uniform shrinkage, leaving hard edges that can protrude into the geometry of the part.
Particle Size Mismatch
Particle size mismatch is another factor that can cause sintering necks. This occurs when the powder is not within a specified particle size range, or when there is an uneven distribution of particle sizes. As such, this can lead to a surface topography with varying levels of embedding depth and can lead to areas where there is a low melting temperature due to a low solids content. This can result in a localized fusion area, known as a sintering neck, near the cooling surface of the part.
Countermeasures for Sintering Neck
There are numerous countermeasures available to address the root cause of sintering neck, including:
• Adjustment of compaction parameters
• Adjustment of sintering time/temperature
• Adjustment of powder properties
• Addition of debinding materials
• Use of additives to improve shelf life or binding strength
• Use of solvents to control necking
• Use of an advanced sintering furnace
By implementing one or more of these countermeasures, manufacturers can ensure that sintering necks are avoided and that the desired quality of the part is achieved.
Conclusion
Sintering neck is a common issue that can occur during powder metallurgy if the parts are not properly prepared and processed. If left unaddressed, sintering neck can lead to poor part quality and even product failure. However, by understanding the root causes and implementing the proper countermeasures, this issue can be avoided. By doing so, manufacturers can ensure that their parts are of the highest quality and reliability.