Metallography of 20CrNi2Mo after Carbon Nitride Diffusion and Low Temperature Annealing
Metallography is the study of metal structures, primarily at the microscopic level, to understand the behavior of metals in various conditions. In this experiment, the metallography of 20CrNi2Mo after carbon nitride diffusion and low temperature annealing was investigated. The metal was heated to 860-900oC and then held at this temperature for one hour. After this treatment, the metal was quickly cooled below 500oC and heated to 600-620oC for one hour. This low temperature annealing was conducted to improve the mechanical properties and toughness of the metal.
The first step in the metallographic examination was to prepare the metal specimen. The specimen was cleaned with a standard solution to remove any oxides and other surface contaminants. Then the specimen was cut into thin slices and mounted in an epoxy resin to prepare it for viewing. After mounting, the specimen was ground, polished and etched with a reagent to reveal the microstructural features of the metal.
The results of the examination showed that the carbon nitride diffusion treatment caused a significant increase in the grain size of the metal. The grain sizes observed were much larger than before the treatment. This was due to the decomposition of the nitride scale and the subsequent grain growth that occurred during the diffusion in the metal. Additionally, the low temperature annealing had an additional effect of reducing the grain size of the metal.
In the metallographic examination of the metal, a two-phase microstructure was observed. The two-phase microstructure consisted mainly of an α-ferrite phase and a martensite phase. The α-ferrite phase consisted of fine grains, while the martensite phase had larger grains with a dendritic structure. The martensitic phase was more prevalent towards the surface of the metal where it was exposed to the heat treatment.
The micrographs also revealed a number of features associated with the grain structure of the metal. There were areas of discontinuity in the grain structure and a number of twins were observed in the ferrite phase. Additionally, some grain boundary sliding and deformation of boundaries was observed as a result of the diffusion process. This was due to the high diffusion rate of the carbon nitrogen species during the low temperature annealing process.
Overall, the metallographic examination of the 20CrNi2Mo after carbon nitride diffusion and low temperature annealing revealed a two-phase microstructure composed of α-ferrite and martensite grains. The diffusion process caused a significant increase in the grain size of the metal, with the martensite phase being the most prevalent phase at the surface of the metal. Additionally, the low temperature annealing process had a further effect on the grain structure of the metal, causing grain boundary deformation and discontinuities in the grain structure.