The microstructure of AISI4140 ZG30CrNiMo alloy steel under normalizing, tempering, and annealing treatments is characterized through optical microscopy and scanning electron microscopy. The results show that when normalizing and tempering, the microstructure of AISI4140 ZG30CrNiMo alloy steel consisted of evenly distributed and well-formed spheroidal carbide grains. The grain size of the spheroidal carbides is relatively uniform in size and there were some small inclusions present. Meanwhile, the matrix grains were more refined after heat treatments, indicating a more refined grain size distribution. After annealing, there were more and larger carbide particles present in the microstructure. In the matrix, there were a few tempered martensite particles which were large in size and a few small particles of untempered martensite, bainite, and ferrite.
The optical micrographs of the AISI4140ZG30CrNiMo alloy steel under normalizing, tempering, and annealing treatments also showed some differences in the microstructure. Under normalizing and tempering heat treatments, the matrix grains were more refined with a fine uniform grain size distribution. In addition, the spheroidal carbides were evenly distributed and the sizes of the carbides were uniform. After annealing, the grain structure of the AISI4140ZG30CrNiMo alloy steel became coarser with the formation of tempered martensite particles in the matrix, along with small untempered martensite, bainite and ferrite particles, which were randomly distributed.
The results of the scanning electron microscope (SEM) images of the AISI4140ZG30CrNiMo alloy steel under normalizing, tempering, and annealing treatments showed some structural changes. After normalizing and tempering, the microstructures were composed of more refined matrix grains and the spheroidal carbides grains were uniform in size. After the annealing treatment, both the matrix grain size and the distribution of the spheroidal carbides were coarser and there were a few tempered martensite particles among small particles of untempered martensite, bainite, and ferrite.
In conclusion, the microstructural and optical properties of the AISI4140ZG30CrNiMo alloy steel changed when exposed to different heat treatments. After normalizing and tempering treatments, the matrix structures were refined and with an even distribution of uniformly sized spheroidal carbides. After annealing treatment, the grain structures of the alloy steel were coarser with the presence of larger particles of tempered martensite particles. The presence of small untempered martensite, bainite and ferrite particles were also observed in the microstructures. Thus, this study has effectively demonstrated how microstructural changes occur in the AISI4140 ZG30CrNiMo alloy steel when it is exposed to different heat treatments.