The microstructure of 38CrMoA1 (ion nitrided) was analyzed by optical microscopy. The microstructure consists of martensite, carbides, and carbide networks in the matrix. The carbides have an approximate diameter of 0.2 to 0.4 µm, and the majority of them appear to have a plate-like morphology, but some are spherical and rod-like in shape. The carbide networks are arranged in a lattice-like pattern, with some portions having a slightly distorted structure.
Martensite is present in the shape of lath-like and blocky structures. The lath-like martensite is aligned in a regular pattern, and the blocky martensite is more dispersed in the matrix, often overlapping with the carbide networks. The martensite appears to be mostly group A, although B and C phases are also present.
The matrix is ferrite in composition, and has a very fine grain size of approximately 0.1 µm, as observed by light microscopy. The matrix grains show some variation in their orientation, and the grain boundaries appear to be discontinuous, which indicates the presence of an interfacial alloying layer.
The presence of the martensite and carbide networks, as well as the fine grain size of the matrix and the presence of an interfacial alloying layer, suggest that the ion nitrided sample has undergone a rapid quenching and tempering process, possibly at a high enough temperature to form a martensitic/retained-austenitic microstructure.
The sample was further analyzed by scanning electron microscopy (SEM). The SEM images reveal that the martensite is composed of small flakes, which align with the grain boundaries, indicating their involvement in the martensitic transformation process. The SEM images also show that the carbides are distributed in the matrix with a dispersed distribution.
The 38CrMoA1 (ion nitrided) sample shows evidence of having undergone a rapid quenching and tempering process. The presence of lath-like and blocky martensite, carbide networks, and an interfacial alloying layer indicate that such a process has been successful in forming a martensitic/retained-austenitic microstructure. The SEM images show that the carbides are distributed in the matrix with a dispersed distribution, and that the martensite is composed of small flakes, which align with the grain boundaries. These observations suggest that the ion nitrided sample has undergone a successful quenching and tempering process, which has led to the desired microstructure.